Download | - View final version: A method for the identification of the mono-O-methylglucoses (PDF, 391 KiB)
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DOI | Resolve DOI: https://doi.org/10.1139/v53-110 |
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Author | Search for: Lemieux, R. U.1; Search for: Bauer, H. F.1 |
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Affiliation | - National Research Council of Canada. Prairie Regional Laboratory
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Format | Text, Article |
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Abstract | Periodate oxidation of any one mono-O-methylglucopyranose and alkaline hydrolysis of the product yields a substance which can be positively distinguished by paper chromatography from the products formed under the same conditions from the other mono-O-methylglucopyranoses. Thus, the components of a mixture of the mono-O-methylglucopyranoses can be readily identified. The method appears useful for the identification of di-O-methylglucoses. Reduction with sodium borohydride prior to periodate oxidation renders the method useful for the identification of tri-O-methylglucoses. The potential value of the method, which can be used on a microscale, is illustrated by an application to the characterization of the O-methylglucoses derived from a water-soluble O-methyl-cellulose |
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Publication date | 1953-09-01 |
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Publisher | Canadian Science Publishing |
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In | |
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Language | English |
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Peer reviewed | Yes |
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NRC number | NRCC 3044 |
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Export citation | Export as RIS |
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Report a correction | Report a correction (opens in a new tab) |
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Record identifier | 6be3eb69-267d-4ae1-9826-01b73e861757 |
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Record created | 2023-09-14 |
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Record modified | 2024-05-03 |
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