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Headspace single-drop microextration for the detection of organotin compounds

From National Research Council Canada

DOIResolve DOI: https://doi.org/10.1016/j.talanta.2003.11.035
AuthorSearch for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-6896-8603; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-2377-2615
Affiliation
  1. National Research Council of Canada. NRC Institute for National Measurement Standards
FormatText, Article
Subjectliquid–liquid extraction; gas chromatography; supercritical fluid extraction
Abstract
The performance of single-drop microextraction (SDME), coupled with gas chromatography/mass spectrometry, was assessed for the determination of tributyltin compounds in water and solid samples. Experimental parameters impacting the performance of SDME, such as microextraction solvent and sampling and stirring time, were investigated. Analytical results obtained by SDME were compared with those generated by conventional solid phase microextraction (SPME) and liquid–liquid extraction (LLE) for the determination of TBT in PACS-2 sediment certified reference material (CRM).
Publication date
In
  • Talanta 63, no. 3: 555–560.
LanguageEnglish
Peer reviewedYes
NRC numberNRC-INMS-459
NPARC number8897410
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Record identifierbba4705f-4b34-4f19-a924-f80d09661390
Record created2009-04-22
Record modified2024-08-12
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