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Microwave-assisted Kochetkov amination followed by permanent charge derivatization : A facile strategy for glycomics

From National Research Council Canada

DOIResolve DOI: https://doi.org/10.1039/C0CC01732A
AuthorSearch for: 1; Search for: ; Search for: 1; Search for: 1
Affiliation
  1. National Research Council of Canada. NRC Institute for Biological Sciences
FormatText, Article
Abstract
We report a simple and rapid microwave-assisted method for the preparation of oligosaccharide-glycosylamines, followed by labelling with tris(2,4,6-trimethoxyphenyl)phosphonium acetic acid N-hydroxysuccinimide ester. The facile strategy introduced a permanent charge at the reducing end of the oligosaccharide. In combination of MALDI-MS, the detection limit for maltoheptaose was as low as 2 fmol μL⁻¹.
Publication date
In
  • Chemical Communications 46, no. 39 (21 October 2010): 7424–7426.
LanguageEnglish
Peer reviewedYes
NPARC number17400938
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Record identifiercb27f614-7964-42aa-b071-ef247321d885
Record created2011-03-25
Record modified2020-04-17
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